2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone (2HB-5NPH) was synthesized and its application to the spectrophotometric determination of iron was studied. The reagent reacts with iron in the pH range 6.0-7.5 to form a yellow coIored 1:2 chelate which is very stable in methanol solution. Beer's law is obeyed in the concentration range 0.05��2.0 ${\mu}gmL^{-1}$ iron and separation procedure using a short column filled with Amberlite XAD-7 nonionic chelating resin is proposed for the spectrophotometric determination of traces of iron. The influence of several ions as interference was discussed. The separation of Fe(III) ion from the mix-ture solution were carried out with the buffer solution (pH 5.0) and 0.25M HCl as eluents.
Citing 'Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin
'
@article{ JCGMDC_1999_v43n5_522}
,title={Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin}
,volume={5}
, number= {5}
, journal={Journal of the Korean Chemical Society}
, publisher={Korean Chemical Society}
, author={Chan Il, Park
and
Byung Doo, Chung
and
Duck Chae, Jung
and
Ki Won, Cha}
, year={1999}
, month={Oct}
TY - JOUR
T2 - Journal of the Korean Chemical Society
AU - Chan Il, Park
AU - Byung Doo, Chung
AU - Duck Chae, Jung
AU - Ki Won, Cha
SN - 1017-2548
TI - Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin
VL - 43
PB - Korean Chemical Society
PY - 1999
ER -
Chan Il, P.
,
Byung Doo, C.
,
Duck Chae, J.
,
&
Ki Won, C.
( 1999).
Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin.
Journal of the Korean Chemical Society,
43
(5)
Korean Chemical Society.
Chan Il, P
,
Byung Doo, C
,
Duck Chae, J
,
&
Ki Won, C
1999,
Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin,
Journal of the Korean Chemical Society,
vol. 5,
no. 5,
[1]
P Chan Il
,
C Byung Doo
,
J Duck Chae
,
and
C Ki Won
,
“Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin”,
Journal of the Korean Chemical Society,
vol. 5,
no. 5,
Oct
1999.
Chan Il, Park
Byung Doo, Chung
Duck Chae, Jung
et al.
“Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin”
Journal of the Korean Chemical Society,
5.
5
1999:
Chan Il, P
,
Byung Doo, C
,
Duck Chae, J
,
Ki Won, C
Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin.
Journal of the Korean Chemical Society
[Internet].
1999.
Oct ;
5
(5)
Chan Il, Park
,
Byung Doo, Chung
,
Duck Chae, Jung
,
and
Ki Won, Cha
,
“Spectrophotometric Determination of Iron with 2-Hydroxybenzaldehyde-5-nitro-pyridylhydrazone after Separation with Amberlite XAD-7 Nonionic Resin.”
Journal of the Korean Chemical Society
5
no.5
()
Oct,
1999):