Powders and thin-layers of a hexagonal titanium disulfide phase have been successfully prepared by modifying the sol-gel process. The reaction of titanium isopropoxide with hydrogen sulfide causes the precipitation of a precursor which was converted to the disulfide on heat-treatment in $H_2S$ at various temperatures depending on the solvent adopted, whereas that of titanium 2-methoxyethoxide with $H_2S$ produces a stable solution which was spin-casted onto silicon substrates followed by thermolysis to give thin films. Upon heat-treatment in $H_2S$, the disulfides show interesting morphological variations in the form of their powders and thin films, which were characterized by SEM and X-ray diffractometer.
Citing 'Modified Sol-Gel Processing for Titanium Disulfide
'
@article{ JCGMDC_1997_v41n3_130}
,title={Modified Sol-Gel Processing for Titanium Disulfide}
,volume={3}
, number= {3}
, journal={Journal of the Korean Chemical Society}
, publisher={Korean Chemical Society}
, author={Yong Bok, Go
and
Young Je, Bae
and
Hee K., Chae}
, year={1997}
, month={Mar}
TY - JOUR
T2 - Journal of the Korean Chemical Society
AU - Yong Bok, Go
AU - Young Je, Bae
AU - Hee K., Chae
SN - 1017-2548
TI - Modified Sol-Gel Processing for Titanium Disulfide
VL - 41
PB - Korean Chemical Society
PY - 1997
ER -
Yong Bok, G.
,
Young Je, B.
,
&
Hee K., C.
( 1997).
Modified Sol-Gel Processing for Titanium Disulfide.
Journal of the Korean Chemical Society,
41
(3)
Korean Chemical Society.
Yong Bok, G
,
Young Je, B
,
&
Hee K., C
1997,
Modified Sol-Gel Processing for Titanium Disulfide,
Journal of the Korean Chemical Society,
vol. 3,
no. 3,
[1]
G Yong Bok
,
B Young Je
,
and
C Hee K.
,
“Modified Sol-Gel Processing for Titanium Disulfide”,
Journal of the Korean Chemical Society,
vol. 3,
no. 3,
Mar
1997.
Yong Bok, Go
and
,
Young Je, Bae
and
,
Hee K., Chae
and
,
“Modified Sol-Gel Processing for Titanium Disulfide”
Journal of the Korean Chemical Society,
3.
3
1997:
Yong Bok, G
,
Young Je, B
,
Hee K., C
Modified Sol-Gel Processing for Titanium Disulfide.
Journal of the Korean Chemical Society
[Internet].
1997.
Mar ;
3
(3)
Yong Bok, Go
,
Young Je, Bae
,
and
Hee K., Chae
,
“Modified Sol-Gel Processing for Titanium Disulfide.”
Journal of the Korean Chemical Society
3
no.3
()
Mar,
1997):
